KMID : 1059519990430010030
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Journal of the Korean Chemical Society 1999 Volume.43 No. 1 p.30 ~ p.35
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Quantitative Analysis of Microcystins in Shellfish Using GC
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Pyo Dong-Jin
Lee Hak-Joo Park Keun-Young Shine Hyun-Du
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Abstract
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It is very difficult to analyze microcystins quantitatively in shellfish, since microcystins in shellfish easily combine with other proteins. Therefore, in this study, we produced 2-methyl-3-methoxy-4-phenylbutyric acid (MMPB) by separating Adda, the most characteristic part of microcystins, from the complexes of proteins and microcystins. MMPB was esterified and used for the quantitative analysis of microcystins in shellfish using GC.
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